UNE EN IEC 62321-11:2024
Determination of certain substances in electrotechnical products - Part 11: Tris(2-chloroethyl) phosphate (TCEP) in plastics by gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS) (Endorsed by Asociación Española de Normalización in March of 2024.)
Determinación de ciertas sustancias en productos electrotécnicos. Parte 11: Tris(2-cloroetil) fosfato (TCEP) en plásticos por cromatografía de gases-espectrometría de masas (GC-MS) y cromatografía líquida-espectrometría de masas (LC-MS) (Ratificada por la Asociación Española de Normalización en marzo de 2024.)
| Standard number: | UNE EN IEC 62321-11:2024 |
| Pages: | 45 |
| Released: | 2024-03-01 |
| Status: | Standard |
UNE EN IEC 62321-11:2024
This part of IEC 62321 specifies two different techniques for the determination of TCEP tris(2-chloroethyl) phosphate (TCEP) in plastics, the GC-MS or LC-MS method; both of which are suitable for quantitative analysis. These two techniques have been evaluated for use with polyurethane, Polyvinyl chloride and polyethylene materials containing TCEP between 200 mg/kg to 2 000 mg/kg. Use of the methods described in International Standard for other polymers and concentration ranges has not been specifically evaluated. These test methods do not apply to plastics materials having a processing temperature higher than 230 !. NOTE TCEP starts thermal decomposition at approximately 230 !. Polymer types which have a processing temperature into shapes of plastics (e.g. pellets, moulded parts, or sheets etc.) not exceeding the decomposition temperature can contain TCEP. Py-TD-GC-MS is another technique, suitable for the screening of TCEP in plastics (See Annex A).
