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Homepage>ASTM Standards>77>77.120>77.120.10>ASTM E3061-17 - Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance Based Method)
Released: 15.01.2017

ASTM E3061-17 - Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance Based Method)

Standard Test Method for Analysis of Aluminum and Aluminum Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance Based Method)

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Standard number:E3061-17
Released:15.01.2017
Status:Active
Pages:11
Section:03.05
Keywords:26.1 The precision of this test method is based on an interlaboratory study conducted in 2015. Eleven laboratories tested 30 different samples, at both high and low composition levels, for up to 32 elements. Every test result represents an individual determination. All participants provided test results in triplicate. Practice was followed for the design and analysis of the data; the details are given in . Supporting data have been filed at ASTM International Headquarters and may be obtained by requesting Research Report . Contact ASTM Customer Service at service@astm.org. ; aluminum alloys; ICP; inductively coupled plasma atomic emission spectrometry; performance based method;
DESCRIPTION

1.1 This test method describes the inductively coupled plasma atomic emission spectrometric analysis of aluminum and aluminum alloys for the following elements:

Elements

Application Range, %

Minimum

Maximum

Si

0.02

16.8

Fe

0.02

3.06

Cu

0.005

7.0

Mn

0.003

1.41

Mg

0.006

8.2

Cr

0.004

0.52

Ni

0.004

2.71

Zn

0.02

9.65

Ti

0.009

0.20

Ag

0.003

0.4

As

0.005

0.012

B

0.009

0.027

Ba

0.002

0.03

Be

0.002

0.11

Bi

0.01

0.59

Ca

0.003

0.048

Cd

0.002

0.055

Co

0.002

0.034

Ga

0.01

0.019

Li

0.001

2.48

Mo

0.02

0.15

Na

0.008

0.026

P

0.01

0.025

Pb

0.009

0.51

Sb

0.01

0.28

Sc

0.01

0.065

Sn

0.008

6.28

Sr

0.0008

0.028

Ti

0.005

0.20

Tl

0.009

0.13

V

0.01

0.12

Zr

0.004

0.25

1.2 This test method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this test method to other elements or different composition ranges if method validation, which includes evaluation of method sensitivity and precision and bias (as described in Section 14), is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user should carefully evaluate the validation data against the laboratory’s data quality objectives. Method validation of scope extensions is also a requirement of ISO/IEC 17025.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Safety hazard statements are given in Section 10 and specific warning statements are given in Sections 15, 17, 18, 19, 20 and 21.