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Main page>ASTM Standards>75>75.040>ASTM D4928-26 - Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
Released: 01.07.2026
ASTM D4928-26
Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
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Standard number:
ASTM D4928-26
Released:
01.07.2026
Status:
Active
Pages:
13
Section:
05.02
Keywords:
coulometric; crude oils; homogenization; Karl Fischer; titration; water; water in crude oils;
ASTM number:
ASTM D4928
Supersedes:
D4928-24
DESCRIPTION
1.1 This test method covers the determination of water with true concentration range from 0.07 % to 9.5 % by mass and 0.02 % to 5.00 % by volume in crude oils using Procedures A and B, respectively, and from 0.04 % to 3.75 % by mass or volume for Procedure C. Mercaptan (RSH) and sulfide (S− or H2S) as sulfur are known to interfere with this test method, but at levels of less than 500 μg/g [ppm(m)], the interference from these compounds is insignificant (see Section 6).
Note 1:To accommodate testing variations for Procedure C, refer to Section 16 for valid reporting range of test results.
1.2 This test method is intended for use with standard commercially available coulometric Karl Fischer reagent.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 8.
1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.